Study of the evolution of the ethyl ester content of extra virgin olive oil after one year of storage and its impact on the quality of the oil

Author(s)

Assia Rabeh , Nadia Maata , Ahmed Adlouni ,

Download Full PDF Pages: 102-110 | Views: 497 | Downloads: 141 | DOI: 10.5281/zenodo.4040971

Volume 4 - August 2020 (08)

Abstract

This study was carried out on 86 olive oil samples from the 2016 olive growing season, in three Moroccan regions; eastern region, central region and northern region, by analyzing the free acidity by titrimetric test (ISO 660) and the ethyl ester content by gas chromatography method 3 grams (COI / T.20 / DOC N ° 31 November). The samples were stored under special conditions and the study took place over two periods 6 and 12 months of storage. Taking into account the acidity analysis, the results obtained showed no change after 6 months of storage. We conclude that 17.44% of the samples degrade passing from the extra virgin category to a virgin category. For the ethyl ester content, 4.6% of the samples were degraded after 6 months of storage and 29.06% were degraded after one year of storage. In addition, we observed that the growing region of olive trees has an impact on the free acidity and the ethyl ester content of olive oil. For this criterion, we observed that in the central region of Morocco, the olive oil samples are the least degraded compared to other regions. Thus, concerning the content of ethyl esters, 13% of the samples come from the central region, 37% from the eastern region and 39% from the northern region. On the other hand, for the analysis of the acidity, 8% of the samples come from the center, 30% of the samples come from the oriental and 17.39% of the samples come from the north. So we can conclude that for the conservation of extra virgin olive oil, the olive trees of the central region of Morocco can benefit from a good storage while retaining their high nutritional quality proven by the analysis of acidity and the content of ethyl esters

Keywords

quality, free acidity, ethyl ester, conservation, region.

References

             i.                    Ater, M., Essalouh, L., Ilbert, H., Moukhli, A., Khadari, B. 2015. L’oleiculture au maroc de la prehistoire a nos jours : pratiques, diversite, adaptation, usages, commerce et politiqes. 06-09/03/2015, Chefchaouen (Maroc).

ii.                  Bejaoui, A. M., Sánchez-Ortiz, A., Paz Aguilera, M., Ruiz-Moreno M. J., Sánchez, S., Jiménez, A., Beltrán, G. 2018.  High power ultrasound frequency for olive paste conditioning: effect on the virgin olive oil bioactive compounds and sensorial characteristics, Innovative Food Science & Emerging Technologies. DOI: 10.1016/j.ifset.2018.02.002.

iii.                Biedermann, M., Bongartz, A., Mariani, C., Grob, K. 2008. Fatty acid methyl and ethyl esters as well as wax esters for evaluating the quality of olive oils. Eur Food Res Technol. DOI 10.1007/s00217-008-0907-x.

iv.                Conseil Oléicole International. 2012. Politique- Maroc.

v.                  COI/T.20/Doc. No 31 November 2012. Method of analysis : Determination of the content of waxes, fatty acid methyl esters and fatty acid ethyl esters by capillary gas chromatography using 3 grams of silica.

vi.                Cost, R., Bartolomeo, G., Saija, E., Rando, R., Albergamo, A., and Dugo, G. 2017. Determination of alkyl esters content in pdo extra virgin olive oils from sicily, Journal of Food Quality. DOI: https://doi.org/10.1155/2017/3078105.

vii.              Di Loreto, G., Giansante, L., Alfei, L. B., Di Giacinto. 2014. Alchil esteri ed altri indicatori per la della qualita e della genuinita degli oli extra vergini italiani. Rivista Italiana Delle Sostanze Grasse. January 2014.

viii.            Fortini, M., Migliorini, M., Cherubini, C., Cecchi,  L., Guerrini, L., Masella, P., and  Parenti  A. 2015. Shelf life and quality of olive oil filtered without vertical centrifugation.  European Journal of Lipid Science and Technology. DOI: 10.1002/ejlt.201500229.

ix.                Gomez-Coca, R .B., Fernandes, G. D., Perez-Camino,  M. C., Moreda,  W. 2016. Fatty acid ethyl esters (faee) in extra virgin olive oil: a case study of a quality parameter. LWT - Food Science and Technology. DOI: https://doi.org/10.1016/j.lwt.2015.10.063.

x.                  Grompone, M. A., Callejas, N., Martínez, N.,  Feller, C., Amarillo, M., and Irigaray, B. A. 2016. Variation of the Content of Ethyl Esters in Extra Virgin Olive Oils during Their Shelf Life.  Journal of Food Science and Engineering. Doi: 10.17265/2159-5828/2016.01.003.

xi.                ISO 660. Septembre 2009 (fr). Corps gras d'origines animale et végétale — Détermination de l'indice d'acide et de l'acidité.

xii.              Jimenez-Lopez,  J. C., Kotchoni, S. O.,  Rodríguez-García, M. I.,  Alché, J. D. 2012. Structure and functional features of olive pollen pectin methylesterase using homology modeling and molecular docking methods. J Mol Model. DOI 10.1007/s00894-012-1492-2.

xiii.            Lacoste, F. 2012. Nouveaux critères utilises pour l’évaluation de la qualité de l’huile d’olive vierge extra, Groupe des chimistes. ITERG expertise corps gras. Madrid - Réunion 9 et 10 octobre2012.

xiv.            La Tribune économie et finance, Agriculture : la culture de l’olivier en nette progression au Maroc. Décembre 2016. https://lnt.ma/agriculture-culture-de-lolivier-nette-progression-maroc/.

xv.              Meftah, H., Latrache, H., Hamadi, F., Hanine, H., Zahir, H., El louali, M. 2014. Comparaison des caractéristiques physicochimiques des huiles d’olives issus de différentes zones de la région TadlaAzilal(Maroc) [Comparison of thephysico-chemical characteristics of the olive oil coming fromdifferent zonesin Tadla Azilal area (Morocco)]. J. Mater. Environ. Sci. 2014, 641-646 ISSN: 2028-2508.

xvi.            Pinatel, C., Artaud, J. 2014. Les huiles d’olive vierges françaises : évolution, état des lieux. OCL. Published by EDP Sciences. DOI: 10.1051/ocl/2014022.

xvii.          Rabeh, A., Maata, N., and Adlouni, A.2018. Importance of the ethyl esters analysis in improvement of the moroccan extra virgin olive oil quality evaluation. Am. J. innov. res. appl. sci. 2018; 6(5): 235- 242.

xviii.        Royaume du Maroc haut commissariat au plan, direction régionale d’Oujda,  la région de l’oriental disparités intra-régionales et développement contraste, Juillet 2012. http://www.hcp.ma/regionoriental/docs/ETUDESREGIONALES/disparites_intra_regionales.pdf.

xix.            Squeo, G., Silletti, R., Summo, C.,  Paradiso, V. M., Pasqualone,  A., and Caponio, 2017. F. Fatty acids methyl and ethyl esters behaviour during olives processing by means of technological coadjuvants; tal. J. Food Sci. Vol 29, 2017.

xx.              Tanouti, K., Serghini, H. C., Abid, M., Mihamou, A., Khiar,  M., Hachem, M. E., Bahetta, Y., et Elamrani, A. 2011. Isly huile d’olive vierge analyse des triglycérides et composition en acides gras. Technolab. 2011, volume, n° 23.

Cite this Article: